Analisis Kadar Air pada Susu Bubuk Kemasan Menggunakan Metode Near Infrared Spectroscopy dan Kemometrik
DOI:
https://doi.org/10.19184/pk.v13i2.52517Keywords:
chemometric, gravimetric, moisture content, near infrared spectroscopy (NIR)Abstract
This study aims to evaluate the feasibility of using Near Infrared Spectroscopy (NIR) for measuring moisture content in powdered milk. The experiment involved creating simulated powdered milk samples by spraying water onto packaged milk powder. The moisture content of the samples was then measured using NIR spectroscopy and gravimetry. Results indicate that NIR spectroscopy is an accurate and reliable method for measuring moisture content in powdered milk, with a strong correlation between the two measurement methods. The experiment utilized 18 training samples with water concentrations ranging from 1-9% and 6 test samples with water concentrations of 3-7%. The NIR spectra of the samples were analyzed using three different calibration models: PLS, PCR, and SVR. The PLS model proved to be the most accurate, with an R-squared value of 0.9346 and an RMSE value of 0.4392. The PLS model was then applied to measure the moisture content in three real powdered milk samples. The results showed no significant difference between the moisture content measured by NIR spectroscopy and gravimetry, demonstrating that NIR spectroscopy is a viable method for determining the moisture content of powdered milk in real-world applications.
Downloads
References
[1] Asriati DW, Thamrin I, Ariyanti M, Ardiansyah A. Pengaruh penambahan polifenol terhadap karakteristik milk chocolate couverture dan analog. Jurnal Industri Hasil Perkebunan. 2020; 15(1): 83.
[2] Glatz-Hoppe J, Boldt A, Spiekers H, Mohr E, Losand B. Relationship between milk constituents from milk testing and health, feeding, and metabolic data of dairy cows. Journal of Dairy Science, 2020; 103(11): 10175–10194.
[3] Badan Standardisasi Nasional Indonesia, “Susu bubuk,” accessed July 29, 2024, [Online]. Available from: http://sispk.bsn.go.id/SNI/DetailSNI/9368
[4] Imaniyah INP. Kajian Etnobiologi Asupan Yang Dianjurkan Untuk Ibu Hamil, Pasca Melahirkan, Dan Balita Masyarakat Pulau Bawean Serta Pemanfaatannya Sebagai Buku Ilmiah Populer. Universitas Jember; 2020.
[5] Karlinasari L, Sabed M, Wistara NJ, Purwanto A, Wijayanto H. Karakteristik spektra absorbansi nir (near infra red) spektroskopi kayu acacia mangium willd pada 3 umur berbeda. Jurnal Ilmu Kehutanan, 2014; 6(1): 45.
[6] Krismaningrum A, Rahmadhia SN. Analisis mutu produk akhir pada pengolahan susu kambing peranakan etawa bubuk di cv pqr d.i. Yogyakarta. Agrokompleks, 2023; 23(1): 70–77.
[7] Depkes, Farmakope Indonesia Edisi VI, Kementerian Kesehatan Republik Indonesia; 2020.
[8] Yusaerah N et al., Konsep Dasar Kimia Analitik. PT. Global Eksekutif Teknologi; 2022.
[9] Beć KB, Grabska J, Huck CW. Near-infrared spectroscopy in bio-applications. Molecules, 2020; 25(12): 2948.
[10] Ramjani R. Pigmen Fikoeritrin Dan Aktivitas Inhibitor Tirosinase Dari Ekstrak Rumput Laut Merah. Jakarta: UIN Syarif Hidayatullah; 2019.
[11] Kumala LYP. Penentuan Model Klasifikasi Dan Kandungan Fitokmia Ekstrak Metanol Daun Sambiloto (Andrographis Paniculata) Di Madura, Jember, Malang Menggunakan Metode Nir Dan Kemometrik. Universitas Jember; 2018
[12] Munawar AA, Hasanuddin, Analisis Data Multivariat, Tim Syiah Kuala University Press; 2020.
[13] Ghozali I. Aplikasi Analisis Multivariate Dengan Program IBM SPSS 25 (Edisi 9), Universitas Diponegoro; 2018.
[14] Artanto FA, Fahlevi R, Rachmayani NA. Partial least square-structural equation modeling (pls-sem) pada hubungan kepuasan konsumen terhadap produk. 2021; 10(1): 43–54.
[15] Liland KH, Mevik B-H, Wehrens R, Hiemstra P. Partial least squares and principal component regression. UTC; 2023.
[16] Ginting LM, Sigiro MM, Manurung ED, Sinurjat JJP. Perbandingan metode algoritma support vector regression dan multiple linear regression untuk memprediksi stok obat. Journal of Applied Technology and Informatics Indonesia, 2021; 1(2): 29–34.
[17] Imanningsih, N. Pengaruh suhu ruang penyimpanan terhadap kualitas susu bubuk. Agrointek, 2014; 7(1): 1–5.
[18] AOAC Internasional. Appendix f: guidelines for standard method performance requirements. AOAC official Method of Analysis, 2016: 9: 2–8.
[19] Lakshmanan MK, Chinnu T, Arvamuthan G, Near-infrared reflectance spectroscopy based online moisture measurement in copra. J. Food Process, 2020; 43(3): 13383.
[20] Wulandari L, Idroes R, Rinaldi TRN, Indrayanto G. Profiles of Drug Substances, Excipients, And Related Methodology. 2022 vol. 47, Elsevier Inc., p. 69.
[21] Miller JN, Miller JC. Statistics and Chemometrics for Analytical Chemistry. Pearson Education; 2018.
[22] Tiolina E, Rachbini W. Partial Least Squares (Teori dan Praktek). Tahta Media; 2022.
[23] Zhang F, O'Donnell LJ. Support vector regression. in Machine Learning, Elsevier; 2020. pp. 123–140. Available from: doi: 10.1016/B978-0-12-815739-8.00007-9.
Downloads
Published
Issue
Section
License
Copyright (c) 2025 Salma Luthfiana Nurshabira, Ayik Rosita Puspaningtyas, Lestyo Wulandari

This work is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.
e-Journal Pustaka Kesehatan has CC-BY-SA or an equivalent license as the optimal license for the publication, distribution, use, and reuse of scholarly work. Authors who publish with this journal retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution-ShareAlike 4.0 International License that allows others to share the work with an acknowledgment of the work's authorship and initial publication in this journal.